Study of the complexes of iron(II) dicyanamide and isothiocyanate with 2-(2-tert-butyltetrazol-5-yl)pyridine

Shakirova O. G.; Lavrenova L. G.; Kuratieva N. V.; Bogomyakov A. S.; Sheludyakova L. A.; Mosalkova A. P.; Grigoriev Yu. V.

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Study of the complexes of iron(II) dicyanamide and isothiocyanate with 2-(2-tert-butyltetrazol-5-yl)pyridine

机译：用2-（2-叔丁基四唑-5-基）吡啶的铁（II）二氰胺和异硫氰酸酯的复合物研究

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Iron(II) dicyanamide and isothiocyanate compounds with 2-(2-tert-butyltetrazol-5-yl)pyridine (L) of the composition [FeL2(C2N3)(2)]aEuro cent 2H(2)O (I) and [FeL2(NCS)(2)]H2O (II) are synthesized and studied. The compounds are examined using powder and single crystal XRD (for I), electron (diffuse reflectance spectra) and IR spectroscopy, static magnetic susceptibility. The analysis of the dependence mu(eff)(D cent) indicates that the exchange interactions of antiferromagnetic nature appear between the iron(II) ions at temperatures below 50 K.

机译：铁（II）二氰胺和异硫氰酸酯化合物，其中组合物的2-（2-叔丁基四唑-5-基）吡啶（L）[FEL2（C2N3）] Aeuro·2H（2）O（I）和[ 合成和研究Fel2（NCS）（2）H 2 O（II）。使用粉末和单晶XRD（用于I），电子（漫反射谱）和IR光谱，静态磁化率检查化合物。依赖mu（eff）（d ceng）的分析表明反铁磁性性质的交换相互作用在低于50k的温度下的铁（II）离子之间。

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来源
《Journal of structural chemistry》 |2017年第5期|共7页
作者
Shakirova O. G.; Lavrenova L. G.; Kuratieva N. V.; Bogomyakov A. S.; Sheludyakova L. A.; Mosalkova A. P.; Grigoriev Yu. V.;
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作者单位

Komsomolsk On Amur State Tech Univ Komsomolsk On Amur Russia;

Russian Acad Sci Nikolaev Inst Inorgan Chem Siberian Branch Novosibirsk Russia;

Russian Acad Sci Nikolaev Inst Inorgan Chem Siberian Branch Novosibirsk Russia;

Novosibirsk Natl Res State Univ Novosibirsk Russia;

Russian Acad Sci Nikolaev Inst Inorgan Chem Siberian Branch Novosibirsk Russia;

Belarusian State Univ Res Inst Phys Chem Problems Minsk BELARUS;

Belarusian State Univ Res Inst Phys Chem Problems Minsk BELARUS;

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正文语种 eng
中图分类结构化学;
关键词
synthesis; coordination compounds; iron(II); 2-(2-tert-butyltetrazol-5-yl)pyridine; structure; magnetic properties;

机译：合成;配位化合物;铁（II）;2-（2-叔丁基四唑-5-基）吡啶;结构;磁性;

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1. Study of the complexes of iron(II) dicyanamide and isothiocyanate with 2-(2-tert-butyltetrazol-5-yl)pyridine [J] . Shakirova O. G., Lavrenova L. G., Kuratieva N. V., Journal of structural chemistry . 2017,第5期

机译：用2-（2-叔丁基四唑-5-基）吡啶的铁（II）二氰胺和异硫氰酸酯的复合物研究
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Study of the complexes of iron(II) dicyanamide and isothiocyanate with 2-(2-tert-butyltetrazol-5-yl)pyridine

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