Crystal structure and thermal properties of Na_2ReCl_6·6H_2O

Shusharina E.; Zadesenets A.; Gromilov S.

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Crystal structure and thermal properties of Na_2ReCl_6·6H_2O

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The crystal structure of Na_2ReCl_6?6H_2O is determined. The crystallographic characteristics are as follows: a = 6.6955(2) ?, b = 7.0926(2) ?, c = 8.3667(3) ?; α = 102.567(1)°, β = 98.853(2)°, γ = 107.236(1)°; V = 360.08(2) ?~3, P-1 space group, Z = 1, d_x = 2.550 g/cm~3. The thermal properties of Na_2ReCl_6?6H_2O are studied in the hydrogen atmosphere. During the thermolysis of Na_2ReCl_6_(0.50)PtCl_6_(0.50)?6H_2O double complex salt in the hydrogen atmosphere, Re_xPt_(1–x) nanocrystalline solid solutions were obtained.

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《Journal of structural chemistry》 |2011年第2期|439-442|共4页
作者
Shusharina E.; Zadesenets A.; Gromilov S.;
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作者单位

A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk;

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原文格式 PDF
正文语种英语
中图分类结构化学;
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rhenium; platinum; thermolysis; crystal chemistry; X-ray diffraction analysis; X-ray powder analysis;

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Crystal structure and thermal properties of Na_2ReCl_6·6H_2O

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